Abstract
Although the phosphor-photomultiplier combination
provides an instrument of great versatility, up to quite
recent times it has been employed almost solely in the
nuclear physics field. This thesis describes some
experiments designed to determine the effectiveness of
the device for the detection and spectrometery of low
energy X-ray quanta such as are employed in X-ray
diffraction work. The present experiments were all
carried out using Copper K radiation (8keV).
A coincidence pair was the principal experimental
arrangement investigated, as this provided a means of
greatly reducing the number of dark noise pulses. A two
channel pulse height analyser was devised to enable the
distribution of the total number of photoelectrons released
in each scintillation to be determined. The single phototube
counter was also investigated and the results obtained
confirm its practibility for X-ray diffraction work
provided photocathodes of high quantum efficiency (15% at
least) are employed. Diffractometer records are included
which illustrate the practical performance of both the single
and coincidence counters.
The absolute accuracies of the measurements made
throughout these experiments are relatively poor since
practically no calibrated test instruments were available
at any stage of the project. However, the satisfactory
overall performance of the equipment is evidenced by the
diffractometer records which generally are aS good, if not
better, than those obtainable on commercial instruments
employing conventional detectors.